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\'02\'04.;}{\levelnumbers\'01;}\fi-360\li3600\jclisttab\tx3600\lin3600 }{\listlevel\levelnfc2\levelnfcn2\leveljc2\leveljcn2\levelfollow0\levelstartat1\levelspace0\levelindent0{\leveltext\leveltemplateid67698715\'02\'05.;}{\levelnumbers\'01;}\fi-180\li4320
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{\leveltext\'02\'05.;}{\levelnumbers\'01;}\fi-180\li4320\jclisttab\tx4320\lin4320 }{\listlevel\levelnfc0\levelnfcn0\leveljc0\leveljcn0\levelfollow0\levelstartat1\levelspace0\levelindent0{\leveltext\'02\'06.;}{\levelnumbers\'01;}\fi-360\li5040
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{\leveltext\leveltemplateid67698715\'02\'02.;}{\levelnumbers\'01;}\fi-180\li2160\jclisttab\tx2160\lin2160 }{\listlevel\levelnfc0\levelnfcn0\leveljc0\leveljcn0\levelfollow0\levelstartat1\levelspace0\levelindent0{\leveltext\leveltemplateid67698703
\'02\'03.;}{\levelnumbers\'01;}\fi-360\li2880\jclisttab\tx2880\lin2880 }{\listlevel\levelnfc4\levelnfcn4\leveljc0\leveljcn0\levelfollow0\levelstartat1\levelspace0\levelindent0{\leveltext\leveltemplateid67698713\'02\'04.;}{\levelnumbers\'01;}\fi-360\li3600
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\fs24\lang2057\langfe1033\cgrid\langnp2057\langfenp1033 {\b\f4\fs48\up6\insrsid8742607 1}{\b\f4\fs48\insrsid8742607 H, }{\b\f4\fs48\up6\insrsid8742607 13}{\b\f4\fs48\insrsid8742607 C, }{\b\f4\fs48\up6\insrsid8742607 15}{\b\f4\fs48\insrsid8742607 N, }{
\b\f4\fs48\up6\insrsid8742607 19}{\b\f4\fs48\insrsid8742607 F and }{\b\f4\fs48\up6\insrsid8742607 31}{\b\f4\fs48\insrsid8742607 P
\par 
\par ONE DIMENSIONAL
\par 
\par NMR SPECTROSCOPY
\par }{\b\f4\fs28\insrsid8742607 (Xwinnmr on PC, W2Kpro, version 3.5)
\par }{\b\f4\fs48\insrsid8742607 
\par on 
\par 
\par DPX 200
\par }{\b\f4\fs48\insrsid8742607\charrsid1518156 and
\par DPX 300}{\b\f4\fs48\insrsid8742607 
\par 
\par }{\b\f4\fs28\insrsid8742607  }{\b\f4\fs48\insrsid8742607 
\par 
\par 
\par }{\b\f4\fs48\insrsid12475853 
\par 
\par 
\par }{\b\f4\fs48\insrsid8742607 
\par }{\b\f4\insrsid8742607 Department of Chemistry
\par University of Oslo
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\b\f4\lang1033\langfe1033\langnp1033\insrsid7218633 February 2005}{\b\f4\lang1033\langfe1033\langnp1033\insrsid8742607 
\par }{\b\f4\fs28\lang1033\langfe1033\langnp1033\insrsid1518156 Version 1}{\b\f4\fs28\lang1033\langfe1033\langnp1033\insrsid8742607  }{\b\f4\fs28\ul\lang1033\langfe1033\langnp1033\insrsid8742607 
\par }{\f4\insrsid8742607 (To be used from }{\f4\insrsid7615022 February 2005}{\f4\insrsid8742607 )
\par }{\fs18\insrsid8742607 200}{\fs18\insrsid7615022 5}{\fs18\insrsid8742607 .  \'a9 B. J. Wik, F. Rise and D. Petersen.}{\b\f4\insrsid8742607 
\par }{\b\fs36\up6\insrsid8742607 \page 1}{\b\fs36\insrsid8742607 H NMR at DPX200 and DPX300
\par }{\insrsid8742607 Version 1
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\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 4.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on the }{\b\insrsid8742607 xwin-nmr 3.5 icon}{\insrsid8742607 .
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 5.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
The xwinnmr window comes up
, click with the mouse left button on the top grey bar and move it with the mouse left button still depressed so that upper left corner of the new window coincides with the upper left corner of the screen and release with left button.  The dEfAuLt dataset
 should come up. Dataset:}{\b\insrsid8742607  < dEfAuLt 1 1 C: UIO-username >}{\insrsid8742607  (C: can be substituted by M:) should be shown under the menu bar. Go to point 8 if default comes up.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 6.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If no default dataset comes up click on }{\b\insrsid8742607 File}{\insrsid8742607  followed by }{\b\insrsid8742607 search}{\insrsid8742607 .  Select any dataset, click on }{\b\insrsid8742607 Append}{\insrsid8742607  and }{\b\insrsid8742607 Apply}{
\insrsid8742607 .  Don}{\insrsid7218633 \rquote t do anything with the dataset,}{\insrsid8742607  this procedure is performed only to allow to perform point 8 below.}{\fs20\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 7.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 edc}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   (edit current dataset).
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\b\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 8.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\b\insrsid8742607 NAME}{
\insrsid8742607 \tab \tab Type in your journal number and/or short name in the upper small window followed by }{\b\f3\fs28\insrsid8742607 \'bf}{\f3\fs28\insrsid8742607 \'2e\'20\'20}{\insrsid8742607 A good name is of the form:  }{\b\insrsid8742607 FR5043II
}{\insrsid8742607  (Frode Rises synthesis 5043 product number two).  }{\fs20\insrsid8742607 Use your initials from your name in front of the file name to ensure that Dirk a
nd Frode can identify the owner of the file   The name must not contain any of the characters: !"#$>&/()=?`^*@\'a8,:;\'a7' '\}\{\'e4\'f6\'e5][ or other curious characters you might find on the keyboard.  _ - and . might be used. 
\par }\pard \qj \fi360\li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\b\lang1033\langfe1033\langnp1033\insrsid8742607 EXPNO\tab \tab \tab 1
\par PROCNO\tab \tab \tab 1
\par DU\tab \tab \tab \tab }{\b\lang1033\langfe1033\langnp1033\insrsid7218633 D}{\b\lang1033\langfe1033\langnp1033\insrsid8742607 :}{\fs20\lang1033\langfe1033\langnp1033\insrsid8742607 
\par }{\b\insrsid8742607 USER\tab \tab \tab \tab UIO-username\tab \tab \tab }{\insrsid8742607 (your uio user name)}{\b\insrsid8742607 
\par TYPE\tab \tab \tab \tab nmr}{\fs20\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 9.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Click on }
{\b\insrsid8742607 save }{\insrsid8742607 with the left mouse button.  }{\fs20\insrsid8742607 The first time you log in as yourself you get an xwinnmr window missing some functional  \'93buttons\'94 in the lower part. Click on }{\b\fs20\insrsid8742607 
display}{\fs20\insrsid8742607  followed by }{\b\fs20\insrsid8742607 options}{\fs20\insrsid8742607  and }{\b\fs20\insrsid8742607 user interface}{\fs20\insrsid8742607 .  A new window comes up, select }{\b\fs20\insrsid8742607 extended}{\fs20\insrsid8742607 
 and set }{\b\fs20\insrsid8742607 zgsafety}{\fs20\insrsid8742607  to }{\b\fs20\insrsid8742607 OFF}{\fs20\insrsid8742607 , and then click on }{\b\fs20\insrsid8742607 apply}{\fs20\insrsid8742607 
.  The xwinnmr window closes and comes up again with all options.  }{\b\fs20\insrsid8742607 File}{\fs20\insrsid8742607  and }{\b\fs20\insrsid8742607 exit}{\fs20\insrsid8742607  to close the user interface.
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid10187803 \hich\af0\dbch\af0\loch\f0 10.\tab}}\pard \ql \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0\pararsid5461176 {
\fs20\insrsid10187803 If you have a big grey area }{\fs20\insrsid5461176 on the left side of the Xwinnmr window you have the standard user interface. This manual is written based on the extended user interface. To change to the extended, do as follows:
\line - Select: }{\b\fs20\insrsid5461176\charrsid5461176 Display}{\fs20\insrsid5461176  => }{\b\fs20\insrsid5461176\charrsid5461176 Options}{\fs20\insrsid5461176  => }{\b\fs20\insrsid5461176\charrsid5461176 User interface}{\b\fs20\insrsid5461176  }{
\fs20\insrsid5461176 fro}{\fs20\insrsid5461176\charrsid5461176 m the menu}{\fs20\insrsid5461176 .\line - Under User interface in the window that comes up, select }{\b\fs20\insrsid5461176\charrsid5461176 extended}{\fs20\insrsid5461176 .\line - Press }{
\b\fs20\insrsid5461176\charrsid5461176 APPLY}{\b\fs20\insrsid5461176 \line - }{\fs20\insrsid5461176\charrsid5461176 Select }{\b\fs20\insrsid5461176 File => Exit}{\fs20\insrsid5461176\charrsid5461176  to exit the user interface window.
\par }\pard \ql \li720\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin720\itap0\pararsid5461176 {\fs20\insrsid5461176\charrsid5461176 You should now see more buttons in the Xwinnnmr window}{\fs20\insrsid5461176 .\line }{
\fs20\insrsid5461176\charrsid5461176 
\par {\listtext\pard\plain\lang1044\langfe1033\langnp1044\insrsid8742607 \hich\af0\dbch\af0\loch\f0 11.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {
\lang1044\langfe1033\langnp1044\insrsid8742607 Type }{\b\lang1044\langfe1033\langnp1044\insrsid8742607 rpar PROTON}{\b\f3\fs28\insrsid8742607 \'bf}{\lang1044\langfe1033\langnp1044\insrsid8742607  }{\b\lang1044\langfe1033\langnp1044\insrsid8742607  }{
\lang1044\langfe1033\langnp1044\insrsid8742607  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\lang1044\langfe1033\langnp1044\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 12.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Press }{
\b\insrsid8742607 copy all}{\insrsid8742607  with the mouse left button.  
\par }\pard \qj \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 13.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 getprosol}{\b\f3\fs28\insrsid8742607 \'bf\tab }{\b\insrsid8742607 (don\rquote t forget, IMPORTANT!)}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 14.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Click on 
}{\b\insrsid8742607 Windows}{\insrsid8742607  in upper right corner of the main window and click left mouse button on }{\b\insrsid8742607 lock}{\insrsid8742607 .  The Lock display comes up, move it to the right of the screen with the mouse, click with th
e left mouse button on the upper part of the window and move/shrink the window.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 15.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf}{\fs28\insrsid8742607  }{\insrsid8742607  (initialize interface). The computer checks that all electronic connections are up and running.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 16.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press the }{\b\insrsid8742607 Spin on/off}{\insrsid8742607  button to off and press then the }{\b\insrsid8742607 Lock on/off }{\insrsid8742607 button to off and finally the }{\b\insrsid8742607 LIFT on/off}{\insrsid8742607 
 button to on the shim console, the standard sample comes up.  Change sample and adjust the height of the new tube with the big adjustment TUBE and put the sample on top of the magnet.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 17.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Press }{
\b\insrsid8742607 LIFT on/off }{\insrsid8742607 to off, sample goes down in the magnet.  Press the }{\b\insrsid8742607 Spin on/off}{\insrsid8742607  button to on.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 18.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 rsh}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  }{\b\insrsid8742607  }{\insrsid8742607  Read shim and select a shim file, for instance, by pressing left mouse button on }{\b\insrsid8742607 QNP.}{\b\insrsid7218633 040824}{
\b\insrsid8742607 .luf }{\insrsid8742607 (always the first file on the list, Dirk periodically updates this).  If the QNP probe is not in the magnet select another shim file with the name BBI/bbi in the filename.  }{\fs20\insrsid8742607 
If you want to save a personal shim file the }{\b\fs20\insrsid8742607 wsh}{\fs20\insrsid8742607  command can be used, do not write on top of existing parameter sets please.  }{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 19.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 lock}{\b\f3\fs28\insrsid8742607 \'bf}{\fs28\insrsid8742607  }{\b\insrsid8742607  }{\insrsid8742607 
A list of solvents comes up - choose your solvent by clicking with left mouse button.  Watch the lock display during the automatic locking procedure.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 20.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Watch to see if the light on }{\b\insrsid8742607 Spin on/off}{\insrsid8742607  is on permanently.  If off click on.  If blinking - wait 30 seconds to see if it comes on.  Check sample height in spinner if not working.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 21.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press LOCK GAIN and use the wheel in order to adjust the lock signal to the upper horizontal line in lockdisplay. 
\par }\pard \qj \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 22.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Press }{
\b\insrsid8742607 Onaxis}{\insrsid8742607  on shim console if no light on that button.  There is no Onaxis button on the DPX 300.Press }{\b\insrsid8742607 STD BY}{\insrsid8742607  instead. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 23.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Press }{
\b\insrsid8742607 Z}{\b\up6\insrsid8742607 1}{\insrsid8742607  (}{\b\insrsid8742607 Z}{\insrsid8742607  on DPX300) on shim console and turn the wheel slowly in one or the other direction.  The purpose is to get the lock signal higher
 in the lock display window.  It is best to perform the shim process about 80> height. If the lock signal goes above the top of the lock display press STD BY and then press LOCK GAIN and move the lock signal down with the wheel.  Then press STD BY again a
nd repeat the Z1 shimming.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 24.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Press }{
\b\insrsid8742607 Z}{\b\up6\insrsid8742607 2}{\insrsid8742607  on shim console and shim with the wheel until the lock signal does not move any further.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 25.\tab}}\pard \qj \fi-360\li720\ri0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Continue with }{
\b\insrsid8742607 Z}{\b\up6\insrsid8742607 1}{\insrsid8742607  (}{\b\insrsid8742607 Z}{\insrsid8742607  on DPX300) and }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 2}{\insrsid8742607 
 alternating until the lock signal is not getting higher. If necessary use }{\b\insrsid8742607 lock gain}{\insrsid8742607  on shim panel if the lock signal comes to the top of the lock display.  Click on }{\b\insrsid8742607 Lock gain}{\insrsid8742607 
 and use the wheel to take the signal down. Press }{\b\insrsid8742607 STD BY}{\insrsid8742607  and }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 1 }{\insrsid8742607 (}{\b\insrsid8742607 Z }{\insrsid8742607 on DPX300)}{\up6\insrsid8742607  }{
\insrsid8742607  or }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 2 }{\insrsid8742607 to get back to shimming. (If you want the instrument to perform autoshim - press }{\b\insrsid8742607 STD BY}{\insrsid8742607  and }{\b\insrsid8742607 Autoshim}{
\insrsid8742607 .  When you want the instrument to stop shimming press }{\b\insrsid8742607 STD BY}{\insrsid8742607  again.  You can run the experiment with the autoshim on. Finish the shim procedure by adjusting }{\b\insrsid8742607 Z}{
\b\super\insrsid8742607 1}{\insrsid8742607 .
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 26.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 rga}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   \tab \tab Receiver gain adjustment is performed, wait until message \'93rga finished\'94 is seen.  }{\fs20\insrsid8742607 If error messages appears type }{\b\fs20\insrsid8742607 ii}{
\b\f3\fs20\insrsid8742607 \'bf\'20}{\fs20\insrsid8742607 (initialize interface), if needed repeat the ii process two or three times.  The instruments adjusts the \'93intensity\'94 received signal depending upon the sample concentration.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 27.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 ns}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  \tab Number of scans.  }{\fs20\insrsid8742607 16 is default,  you have to put in another number if you wish.  Type }{\b\fs20\insrsid8742607 d1}{\fs20\insrsid8742607 
 to see the relaxation delay between each pulse.  }{\b\fs20\insrsid8742607 d1}{\fs20\insrsid8742607  must be very long if you want correct/exact integration.  Type in a new number (in seconds - for instance 10) and use the }{\b\f3\fs20\insrsid8742607 \'bf
}{\fs20\insrsid8742607  key.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 28.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 expt}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   \tab This tells you how long time the experiment will take.  Important if you run an experiment over night.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 29.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 zg}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  \tab \tab Zero go, removes old content (if any) from the experiment and starts the experiment.  }{\fs20\insrsid8742607 Type }{\b\fs20\insrsid8742607 ii}{\b\f3\fs20\insrsid8742607 \'bf
\'20}{\fs20\insrsid8742607 if error messages appears followed by a new }{\b\fs20\insrsid8742607 zg}{\b\f3\fs20\insrsid8742607 \'bf}{\fs20\insrsid8742607   when}{\b\fs20\insrsid8742607  ii}{\fs20\insrsid8742607  is finished. }{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 30.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
You can watch the individual scans by typing}{\b\insrsid8742607  acqu}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .  Press \'93}{\b\insrsid8742607 Ctrl-Alt-Del}{\insrsid8742607 \'94 and then click \'93}{\b\insrsid8742607 lock computer}{
\insrsid8742607 \'94 if the experiment takes some time.  }{\fs20\insrsid8742607 Since you are running with your uio account ev
eryone can take a look at your home directory and copy, read and delete whatever they want if you leave the computer without performing }{\insrsid8742607 \'93}{\b\insrsid8742607 lock computer}{\insrsid8742607 \'94}{\fs20\insrsid8742607 .  }{
\insrsid8742607 \'93}{\b\insrsid8742607 Lock computer}{\insrsid8742607 \'94}{\fs20\insrsid8742607  closes your session for other users.  Press }{\insrsid8742607 \'93}{\b\insrsid8742607 Ctrl-Alt-Del}{\insrsid8742607 \'94}{\fs20\insrsid8742607 
 on the keyboard and type in
 your uio password to open the screen again.  If you do not return to the instrument when your time is over the next user can boot the computer to get access to the instrument and you will loose your data if the experiment is not finished at that time.

\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 31.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 efp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
  when not acquiring anymore - to perform exponential multiplication and Fourier transformation of the data.  It can be hard to know when the spectrometer is done acquiring if you are not watching carefully.  No data are stored automatically whi
le running.  If you want to see a spectrum before completed experiment type }{\b\insrsid8742607 tr}{\b\f3\fs28\insrsid8742607 \'bf\'20}{\insrsid8742607 (transfer from memory to disk) and do }{\b\insrsid8742607 efp}{\b\f3\fs28\insrsid8742607 \'bf}{
\insrsid8742607  when the tr process is finished.  You then have to }{\b\insrsid8742607 efp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   again at the end of the experiment if you want to make use off all the scans.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 32.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 apk}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 \tab the computer performs automatic phasing.  Type }{\b\insrsid8742607 abs}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
  (automatic baseline correction) if baseline is distorted.   }{\b\insrsid8742607 apks}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 \tab is an alternative if apk behaves badly.  }{\fs20\insrsid8742607 
Manual phasing is also possible.  Look at the menu to the left.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 33.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Expand t
he area where you have the reference peak (for instance the residual CH [7.24] singlet in CDCl}{\fs20\dn4\insrsid8742607 3}{\insrsid8742607 ).  Put the arrow on the sp
ectrum baseline to the left of the area you want to expand, click with the left and the middle mouse buttons successively.  Move the vertical arrow to the right side, click with middle mouse button to mark the other side and the left mouse button to get t
he pointer back.  Click on the}{\b\f3\fs36\insrsid8742607 \'e0}{\insrsid8742607  button and hold left mouse button pressed down and move the mouse to increase the height.  Click with left mouse button on }{\b\insrsid8742607 calibrate}{\insrsid8742607 
  - put the arrow on top of the peak - click with middle mouse button, new sub menu comes up - type in number (7.24 or other value). Press enter.    
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 34.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Click on}
{\b\insrsid8742607  }{\b\fs28\insrsid8742607 |<>| }{\insrsid8742607 to regain the full spectrum.  Decrease the height if needed with the}{\b\f3\fs48\insrsid8742607 \'e0}{\insrsid8742607  button.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 35.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Expand the spectrum on the screen in preparation for integration.  Put the arrow on the spectrum 
baseline to the left of the area you want to expand, click with the left and the middle mouse buttons successively.  Move the vertical arrow to the right side, click with middle mouse button to mark the other side and the left mouse button to get the pint
er back. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 36.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on the }{\b\insrsid8742607 integrate}{\insrsid8742607  button to enter the integration subroutine. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 37.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Move the pointer to the baseline of the spectrum.  Click with the left button, a new type of arrow appears on the spectrum baseline.  Move the arrow with the mouse (no b
uttons depressed) to the starting point of the first integral from left.  Then press the }{\i\insrsid8742607 middle button}{\insrsid8742607 
  (where you want the first region to start), click then with the middle button on the other side of the peak.  Use the middle button on successive sectio
ns (Before a peak and after).  Click with left button to get out of integral selection mode.  The first region you choose will be set to a value of ONE.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 38.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Use the button: }{\b\f3\fs36\insrsid8742607 \'e0}{\fs36\insrsid8742607  }{\insrsid8742607 under }{\b\insrsid8130040 calibrate}{\insrsid8742607  to adjust sensible integral heights with left mouse button.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 39.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Select a signal which represents a known number of protons by placing the pointer on the signal and press with the left mouse button until you see a white arrow on the top of the integral.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 40.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Click on 
}{\b\insrsid8742607 calibrate}{\insrsid8742607 , a new window appears and type in the number of protons. Press enter.  Remove the star by clicking on a region with no integrals twice with left mouse button.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 41.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Click on 
}{\b\insrsid8742607 return}{\insrsid8742607 .  Click on }{\b\insrsid8742607 save as intreg & return}{\insrsid8742607 .  You don't see the integrals any more but they will appear on the paper.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 42.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type}{
\b\insrsid8742607  f1p}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   to set left ppm value. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 43.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
New long flat window appears, press the mouse left button with the arrow on the gray/brown area on top and drag the window higher up on the screen, let go of the mouse button.  Type in the ppm value you want to have on the left end of the spectrum.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 44.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 f2p}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   to set the right ppm value.    
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 45.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
New long flat window appears, press the mouse left button with the arrow on the gray/brown area on top and drag the window higher up on the screen, let go of the mouse button.  Type in the ppm value (lowest number).
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0\pararsid8657614 {\insrsid8657614 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8657614 \hich\af0\dbch\af0\loch\f0 46.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8657614 Type }{
\b\insrsid8657614\charrsid8657614 edo}{\insrsid8657614  to open the \'93output device parameters\'94 window. In the \'93CURPLOT\'94 and the \'93CURPRINT\'94, select }{\b\insrsid8657614\charrsid8657614 \'93$HP LaserJet 4L\'94}{
\insrsid8657614\charrsid8657614 .}{\insrsid8657614  Now you have selected the laser printer on the side of the screen as output device.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 47.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click with the left mouse button on }{\b\insrsid8742607 utilities}{\insrsid8742607 
.  You are entering a calibration routine for selecting the height of the resonances.  If you don't do this, the largest peak will automatically be scaled to maximum on the paper. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 48.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 pscal global}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 49.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Look at the left side of the spectrum to see if the scale is in cm.  If not cm on the vertical scale on the left you are in absolute mode.  Press the }{\b\insrsid8742607 YU}{\insrsid8742607  button if you are in absolute mode to convert to cm scale.  

\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 50.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press the }{\b\insrsid8742607 CY}{\insrsid8742607  button with the l
eft mouse button.  Threshold line comes up.  Put the threshold on the top of a peak that you want to have at a certain height on the paper. Press left mouse button to set/fix the threshold at this level.  A new window appears.  Enter the height in centime
ter.   Press }{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .  Be aware that the height is not the same on A3 and A4 paper sizes.  Max. height on A4 is 10cm and for A3 18cm.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 51.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Click on 
}{\b\insrsid8742607 MI }{\insrsid8742607 with left mouse button, threshold comes up again.  Put it where you want the peak picking minimum threshold is to be set.  Click with left mouse button.  Click on }{\b\insrsid8742607 MAXI }{\insrsid8742607 
and place the threshold line above the tallest peak you want peak picking for.  (Peaks above this line will not be listed).  Click with left mouse button.  Type }{\b\insrsid8742607 pp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
 if you want the list with Hz and ppm on a separate sheet of paper.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 52.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Click on 
}{\b\insrsid8742607 Return}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 53.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 setti}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\fs28\insrsid8742607 \'20}{\insrsid8742607 to define a title for your spectrum. Type the name you want to give your spectrum, select }{\b\insrsid8742607 save}{\insrsid8742607 
 from the file menu. Exit by choosing }{\b\insrsid8742607 exit}{\insrsid8742607  from the file menu.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 54.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 view}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to get a preview. (}{\b\insrsid8742607 viewx}{\insrsid8742607  gives previews of the command }{\b\insrsid8742607 plotx}{\insrsid8742607  which plots expansions automatically).
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 55.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If you need to correct something type }{\b\insrsid8742607 edg}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 , now you will see a grey window with several grey buttons. Here you can adjust almost everything that is related to plotting.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 56.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If the spectrum looks right, type }{\b\insrsid8742607 plot}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 . The spectrum will now be printed on one of the printers in the NMR lab.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 57.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If you NOW want to run a }{\fs20\up6\insrsid8742607 13}{\insrsid8742607 C experiment on the same sample go to point 8 in the following section for }{\fs20\up6\insrsid8742607 13}{\insrsid8742607 C experiments. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 58.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Eject sample with the }{\b\insrsid8742607 Lift on/off }{\insrsid8742607 button on the shim console and remove your sample from spinner and reinsert the standard sample and lower it by pressing }{\b\insrsid8742607 Lift on/off}{\insrsid8742607  and type }{
\b\insrsid8742607 lock cdcl3}{\insrsid8742607  and see that the instrument locks in the lock window.  Press }{\b\insrsid8742607 Spin on.}{\insrsid8742607  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 59.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 delp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  and a list of all your experiments on the }{\insrsid8657614 D}{\insrsid8742607 
: disk (M: if you run on your home directory) comes up, click on all experiments where there is not said \'93no processed data\'94.  Then click on }{\b\insrsid8742607 execute}{\insrsid8742607 .  Do not click on delete all, you might loose
 all data including acquisition data if you do this.  }{\b\insrsid8742607 delp}{\insrsid8742607  (delete processed data) kills all processed data and helps conserve disk space.  }{\fs20\insrsid8742607 
Please use delp - we are all the time running out of disk space.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 60.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type }{
\b\insrsid8742607 wrd}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   this is the command for writing t
he dataset to another disk.  Usually there is no need for this since USIT is taking backup copies every second from all of the hard disks in the nmr lab.  Go to 62 if you do not want to save the dataset.  Continue as follows if you want a copy on another 
disk.  
\par }\pard \qj \fi360\li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 Enter target data set }{\b\insrsid8742607 NAME:}{\insrsid8742607 \tab \tab }{\b\insrsid8742607 FR5043II}{\b\f3\fs28\insrsid8742607 
\'bf}{\b\insrsid8742607 \tab \tab }{\insrsid8742607 (use your own expname)}{\b\insrsid8742607 
\par }\pard \qj \li720\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin720\itap0 {\insrsid8742607 Enter target data set}{\b\insrsid8742607  EXPNO:\tab 1}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607 \tab \tab \tab }{\insrsid8742607 
(use the expno seen in the top part of the xwinnmr window).
\par Enter target data set }{\b\insrsid8742607 PROCNO:\tab 1}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607 \tab \tab \tab }{\insrsid8742607 (use the procno seen in the top part of the xwinnmr window).
\par }\pard \qj \fi-3600\li4320\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin4320\itap0 {\insrsid8742607 Enter target disk unit }{\b\insrsid8742607 DU}{\insrsid8742607 :\tab }{\b\insrsid8742607 M:}{\b\f3\fs28\insrsid8742607 \'bf}{
\insrsid8742607  \tab The data set will go to your home directory.  }{\fs20\insrsid8742607 The available disks are: C: and M:. }{\insrsid8742607 
\par }\pard \qj \fi360\li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 Enter target user name }{\b\insrsid8742607 USER}{\insrsid8742607 :\tab }{\b\insrsid8742607 UIO-username}{\b\f3\fs28\insrsid8742607 
\'bf}{\b\insrsid8742607  \tab }{\insrsid8742607 (your own uio user name)
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 61.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 The da
taset is now copied.  If you want to move expno 2, 3, 4, 11, 12 or whatever expno you have used - get each dataset in the Xwinnmr window (}{\b\insrsid8742607 re 11}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
 moves expno 11 into the window for instance) and }{\b\insrsid8742607 wrd}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  it away.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 62.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on the }{\b\insrsid8742607 quit}{\insrsid8742607  button in the }{\b\insrsid8742607 lock display}{\insrsid8742607  with the left mouse button.  The next user will not be able to open the lock display if you forget this.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 63.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Type}{
\b\insrsid8742607  kill}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  in the xwinnmr window.  If some xwinnmr processes are running you will get a list.  It is especially important to kill the lock dis
play if it is on the list.  Click on the lock display in the list.  If the lock display is not completely removed before logging out the next user will be unable to open the lock display.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 64.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 
To end the session, press }{\b\insrsid8742607 exit}{\insrsid8742607  under }{\b\insrsid8742607 File}{\insrsid8742607  (left upper corner in main xwinnmr window) and }{\b\insrsid8742607 OK}{\insrsid8742607  in CPR window which appears.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 65.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls1\adjustright\rin0\lin720\itap0 {\insrsid8742607 Select }{
\b\insrsid8742607 log out}{\insrsid8742607  from the start menu to log out of the computer.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 \page }{\b\insrsid8742607 Common errors and how to deal with them.
\par }{\insrsid8742607 
\par }\pard \qj \fi-720\li720\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin720\itap0 {\insrsid8742607 A.\tab The xwinnmr window(s) freezes (especially if you do a mistake when selecting plot
ter/printer/ paper size) and no respond comes when clicking at the various parts of the xwinnmr windows.  Try typing }{\b\insrsid8742607 kill}{\insrsid8742607 
 in the typing area far down in the main xwinnmr window.  If a window with a list of active processes comes up try to click on one of t
hem at time, from the bottom of the list and up, and check after each killing to see if the things behave better.  You will then come back where you were before.
\par 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 B.\tab The computer is locked by another user: 
\par }\pard \qj \li720\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin720\itap0 {\insrsid8742607 Consult the booking list before doing anyth
ing, try to find or call the person if she has gone beyond her time.  If more than 5 minutes past the end of her time boot the computer with the button with the green light on the middle of the computer, and start your own experiment.  Don\rquote 
t boot the computer if the other person is legally running the instrument!!!
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par }\pard \qj \fi-720\li720\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin720\itap0 {\insrsid8742607 C.\tab 
It is impossible to get the lock display up, look at the cabinet door of the spectrometer, instructions for what to do is taped on the door.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 \page }{\b\fs36\up6\insrsid8742607 13}{\b\fs36\insrsid8742607 C NMR at DPX200 and DPX300. 
\par }{\insrsid8742607 Version 1
\par }{\b\fs28\insrsid8742607 If you run the }{\b\fs28\up6\insrsid8742607 13}{\b\fs28\insrsid8742607 C directly after a }{\b\fs28\up6\insrsid8742607 1}{\b\fs28\insrsid8742607 H you can save a lot of time by starting at point 8 below while selecting expno to 2.
}{\fs28\insrsid8742607 
\par }\pard \qj \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 1.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Sit down in front of the instrument.  Move the mouse to remove the screen saver or press a button on the keyboard.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 2.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
user:\tab \tab type your uio: }{\b\insrsid8742607 UIO-username }{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .(similar to UIO-atomsen, UIO-glangli etc)
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 3.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Password:\tab type your uio password \'93}{\b\insrsid8742607 gl@3rd}{\insrsid8742607 \'94}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .}{\b\insrsid8742607   }{\insrsid8742607  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 4.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on the }{\b\insrsid8742607 xwin-nmr 3.5 icon}{\insrsid8742607 .
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 5.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
The xwinnmr window comes up, click with the mouse left button on the top gray bar and move it
 with the mouse left button still depressed so that upper left corner of the new window coincides with the upper left corner of the screen and release with left button.  The dEfAuLt dataset should come up. Dataset:}{\b\insrsid8742607 
 < dEfAuLt 1 1 C: UIO-username >}{\insrsid8742607  (C: can be substituded M:) should be shown under the menu bar. Go to point 8 if default comes up.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 6.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If no default dataset comes up click on }{\b\insrsid8742607 File}{\insrsid8742607  followed by }{\b\insrsid8742607 search}{\insrsid8742607 .  Select any dataset, click on }{\b\insrsid8742607 Append}{\insrsid8742607  and }{\b\insrsid8742607 Apply}{
\insrsid8742607 .  Don\rquote t do anything with the dataset, this procedure is performed only to allow to perform point 8 below.  }{\fs20\insrsid8742607 At this point realize that search can be used to find data sets from the other nmr computers!
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 7.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 edc}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   (edit current dataset).
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 8.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\b\insrsid8742607 
NAME}{\insrsid8742607  Type in your journal number and/or short name in the upper small window followed by }{\b\f3\fs28\insrsid8742607 \'bf}{\f3\fs28\insrsid8742607 \'2e\'20\'20}{\insrsid8742607 A good name is of the form:  }{\b\insrsid8742607 FR5043II}{
\insrsid8742607  (Frode Rises synthesis 5043 product number two).  }{\fs20\insrsid8742607 Use your initials from your name in front of the file name to ensure that Dirk 
and Frode can identify the owner of the file   The name must not contain any of the characters: !"#$>&/()=?`^*@_-\'a8.,:;\'a7' '\}\{\'e4\'f6\'e5][ or other curious characters you might find on the keyboard.  
\par }\pard \qj \fi360\li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\b\insrsid8742607 EXPNO\tab \tab 2 }{\insrsid8742607 (use 2 here if 1 contains another experiment for instance a }{\fs20\up6\insrsid8742607 1}{
\insrsid8742607 H).}{\b\insrsid8742607 
\par }{\b\lang1033\langfe1033\langnp1033\insrsid8742607\charrsid1518156 PROCNO\tab \tab 1
\par DU\tab \tab \tab }{\b\lang1033\langfe1033\langnp1033\insrsid4600484\charrsid1518156 D}{\b\lang1033\langfe1033\langnp1033\insrsid8742607\charrsid1518156 :}{\fs20\lang1033\langfe1033\langnp1033\insrsid8742607\charrsid1518156 
\par }{\b\insrsid8742607 USER\tab \tab \tab UIO-username\tab \tab \tab \tab }{\insrsid8742607 (your uio user name)}{\b\insrsid8742607 
\par TYPE\tab \tab \tab nmr
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 9.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on }{\b\insrsid8742607 save }{\insrsid8742607 with left mouse button.
\par }\pard \qj \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 10.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 rpar C13CPD}{\insrsid8742607  for proton decoupled spectra.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 11.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press }{\b\insrsid8742607 copy all}{\insrsid8742607  with the mouse left button.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 12.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 getprosol}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 13.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on }{\b\insrsid8742607 Windows}{\insrsid8742607  in upper right corner of the main window and click left mouse button on }{\b\insrsid8742607 lock}{\insrsid8742607 
.  The Lock display comes up, move it to the right of the screen with the mouse, click with the left mouse button on the upper part of the window and move/shrink the window.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 14.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf}{\fs28\insrsid8742607  }{\insrsid8742607  (initialize interface).
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 15.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press the }{\b\insrsid8742607 Spin on/off}{\insrsid8742607  button to off and press then the }{\b\insrsid8742607 Lock on/off }{\insrsid8742607 button to off and finally the }{\b\insrsid8742607 LIFT on/off}{\insrsid8742607 
 button on the shim console, the sample comes up.  Change sample and adjust the height of the new tube with the big adjustment TUBE and put the sample on top of the magnet.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 16.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press }{\b\insrsid8742607 LIFT on/off }{\insrsid8742607 to off, sample goes down in the magnet.  Press the }{\b\insrsid8742607 Spin on/off}{\insrsid8742607  button to on.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 17.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
 Type }{\b\insrsid8742607 rsh}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  }{\b\insrsid8742607  }{\insrsid8742607  read shim and select a shim file, for instance, by pressing left mouse button on }{\b\insrsid8742607 qnp.}{\b\insrsid7081987 040828}{
\b\insrsid8742607 .luf }{\insrsid8742607 (Dirk periodically updates this).  }{\ul\insrsid8742607 No need to do this if you just have performed a }{\ul\up6\insrsid8742607 1}{\ul\insrsid8742607 H experiment on the same sample}{\insrsid8742607 .  }{
\fs20\insrsid8742607 If you want to save a personal shim file the wsh command can be used, do not write on top of existing parameter sets please.  }{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 18.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 lock}{\b\f3\fs28\insrsid8742607 \'bf}{\fs28\insrsid8742607  }{\b\insrsid8742607  - }{\insrsid8742607 
a list of solvents comes up - choose your solvent by clicking with left mouse button.  Watch the lock display during the automatic locking procedure.  }{\ul\insrsid8742607 No need to do this if the sample is already locked. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 19.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Watch to see if the light on }{\b\insrsid8742607 Spin on/off}{\insrsid8742607  is on permanently.  If off click on.  If blinking - wait 30 seconds to see if it comes on.  Check sample height in spinner if not working.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 20.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press }{\b\insrsid8742607 Onaxis}{\insrsid8742607  on shim console if no light on that button.  On DPX300 there is no Onaxis button.  Press standby button instead.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 21.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 1}{\insrsid8742607  (}{\b\insrsid8742607 Z}{\insrsid8742607  on DPX300) on shim console and shim slowly with the wheel.  The purpose is to get the lock signal higher in the lock display
 window.  It is best to perform the shim process about 80> height.  If the lock signal goes above the top of the lock screen press STD BY and then LOCK PWR and move the lock signal down with the wheel.  Then press STD BY again and repeat the Z1 shimming. 

\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 22.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 2}{\insrsid8742607  on shim console and shim with wheel.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 23.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Continue with }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 1}{\insrsid8742607  and }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 2}{\insrsid8742607  until lock signal is not getting higher.  Lower }{\b\insrsid8742607 lock gain}{\insrsid8742607 
 on shim panel if the lock signal comes to the top of the lock display.  Click on }{\b\insrsid8742607 Lock gain}{\insrsid8742607  and use the wheel to take the signal down. Press }{\b\insrsid8742607 STD BY}{\insrsid8742607  and }{\b\insrsid8742607 Z}{
\b\up6\insrsid8742607 1}{\insrsid8742607  (}{\b\insrsid8742607 Z}{\insrsid8742607  on DPX300) or }{\b\insrsid8742607 Z}{\b\up6\insrsid8742607 2 }{\insrsid8742607 to get back to shimming. (If you want the instrument to perform autoshim - press }{
\b\insrsid8742607 STD BY}{\insrsid8742607  and thereafter }{\b\insrsid8742607 Autoshim}{\insrsid8742607 .  }{\fs20\insrsid8742607 When you want the instrument to stop shimming press }{\b\fs20\insrsid8742607 STD BY}{\fs20\insrsid8742607 
 again.  You can run the experiment with the autoshim on.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 24.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 rga}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  Receiver gain adjustment is performed, wait until message rga finished is seen.  If error messages appears type }{\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf\'20}{
\insrsid8742607 (initialize interface), if needed repeat the process two or three times.  The instruments adjust the received signal depending upon the sample concentration.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 25.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 ns}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  number of scans.  1024 (1 k) is default,  you have to put in another number if you wish.  Type }{\b\insrsid8742607 d1}{\insrsid8742607 
 to see the relaxation delay between each pulse.  }{\b\insrsid8742607 d1}{\insrsid8742607 
 must be very long if you want correct/exact integration or want to see carbons with no hydrogens attached to them.  Type in a new number (in seconds - for instance 10) and use the }{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  key.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 26.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 expt}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  This tells you how long time the experiment will take.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 27.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 zg}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  Zero go, removes the content from the experiment and starts the experiment.  }{\fs20\insrsid8742607 Type }{\b\fs20\insrsid8742607 ii}{\b\f3\fs20\insrsid8742607 \'bf\'20}{
\fs20\insrsid8742607 if error messages appears followed by a new }{\b\fs20\insrsid8742607 zg}{\b\f3\fs20\insrsid8742607 \'bf}{\fs20\insrsid8742607   when}{\b\fs20\insrsid8742607  ii}{\fs20\insrsid8742607  is finished. }{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 28.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Watch far down on the screen to see how long time to finished experiment, do nothing, you can watch the individual scans by typing}{\b\insrsid8742607  acqu}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 . Press \'93}{\b\insrsid8742607 Ctrl-Alt-Del}{
\insrsid8742607 \'94 and then click \'93}{\b\insrsid8742607 lock computer}{\insrsid8742607 \'94 if the experiment takes some time.  }{\fs20\insrsid8742607 
Since you are running with your uio account everyone can take a look at your home directory and copy, read and delete whatever they want if you leave the computer without performing }{\insrsid8742607 \'93}{\b\insrsid8742607 lock computer}{\insrsid8742607 
\'94}{\fs20\insrsid8742607 .  }{\insrsid8742607 \'93}{\b\insrsid8742607 Lock computer}{\insrsid8742607 \'94}{\fs20\insrsid8742607  closes your session for other users.  Press }{\insrsid8742607 \'93}{\b\insrsid8742607 Ctrl-Alt-Del}{\insrsid8742607 \'94}{
\fs20\insrsid8742607  on the keyboard and type in your uio password to open the screen again.  If you do not r
eturn to the instrument when your time is over the next user can boot the computer to get access to the instrument and you will loose your data if the experiment is not finished at that time.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 29.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 efp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   when not acquiring anymore to Fourier transform 
the data.  It can be hard to know when the spectrometer is done acquiring if you are not watching carefully.  No data are stored automatically while running.  If you want to see a spectrum before completed run type }{\b\insrsid8742607 tr}{
\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 (transfer) and }{\b\insrsid8742607 efp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .  You then have to run }{\b\insrsid8742607 efp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
  again at the end if you want to make use off all the scans.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 30.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 apk}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 \tab the computer performs automatic phasing.  Type }{\b\insrsid8742607 abs}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
  (automatic baseline correction) if baseline is distorted.   }{\b\insrsid8742607 apks}{\b\f3\fs28\insrsid8742607 \'bf\'20}{\insrsid8742607 is an alternative if apk behaves badly.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 31.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Expand the area where you have the reference peak (for instance the CDCl}{\dn4\insrsid8742607 3}{\insrsid8742607  [77.0] triplet in }{\up6\insrsid8742607 13}{\insrsid8742607 
C).  Put the arrow on the spectrum baseline to the left of the area you want to expand, click with the left and the middle mouse buttons successively.  Move the v
ertical arrow to the right side, click with middle mouse button to mark the other side and the left mouse button to get the pointer back.  Click on the}{\b\f3\fs48\insrsid8742607 \'e0}{\insrsid8742607 
 button and hold left mouse button pressed down and move the mouse to increase the height.  Click with left mouse button on }{\b\insrsid8742607 calibrate}{\insrsid8742607 
  - put the arrow on top of the peak - click with middle mouse button, new sub menu comes up - type in number (77.00 or other value). Press }{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .    
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 32.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on}{\b\insrsid8742607  }{\b\fs28\insrsid8742607 |<>| }{\insrsid8742607 to regain the full spectrum.  Decrease the height if needed with the}{\b\f3\fs48\insrsid8742607 \'e0}{\insrsid8742607  button.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 33.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type}{\b\insrsid8742607  f1p}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   to set left ppm value. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 34.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
New long flat window appears, press the mouse left button with the arrow on the gray/brown area on top and drag the window higher up on the screen, let go of the mouse button.  Type in the ppm value you want to have on the left end of the spectrum.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 35.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 f2p}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   to set the right ppm value.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 36.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
New long flat window appears, press the mouse left button with the arrow on the gray/brown area on top and drag the window higher up on the screen, let go of the mouse button.  Type in the ppm value (lowest number).
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 37.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click with the left mouse button on }{\b\insrsid8742607 utilities}{\insrsid8742607 .  You are entering a calibration routine for selecting the height of the resonances.  If you don't do this the largest peak (often the solven
t) will automatically be scaled to maximum on the paper.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 38.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 pscal global}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 39.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Look at the left side of the spectrum to see if the scale is in cm.  If not cm on the scale you are in absolute mode.  Type }{\b\insrsid8742607 a/r}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  }{\b\insrsid8742607  }{\insrsid8742607 or press the }{
\b\insrsid8742607 YU}{\insrsid8742607  button if you are in absolute mode.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 40.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press the }{\b\insrsid8742607 CY}{\insrsid8742607 
 button with the left mouse button.  Threshold line comes up.  Put the threshold on the top of a peak which you want to have at a certain height on the paper.  Press left mouse button to set/fix the threshold at this level.  A
 new window appears.  Enter the height in centimeter.   Press }{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 .  Be aware that the height is not the same on A3 and A4 paper sizes.  Max. height on A4 is 11cm and for A3 18cm.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 41.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on }{\b\insrsid8742607 MI }{\insrsid8742607 with left mouse button, threshold comes up again.  Put it where you want the peak picking minimum threshold is to be set.  Click with left mouse button.  Click on }{\b\insrsid8742607 MAXI }{
\insrsid8742607 and place the threshold line above the tallest peak you want peak picking for.  (Peaks above this line will not be listed).  Click with left mouse button.  Type }{\b\insrsid8742607 pp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
  if you want the list with Hz and ppm on a separate sheet of paper.}{\b\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 42.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on }{\b\insrsid8742607 Return.}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 43.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 setti}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\fs28\insrsid8742607 \'20}{\insrsid8742607 to define a title for your spectrum. Type the name you want to give your spectrum, select }{\b\insrsid8742607 save}{\insrsid8742607 
 from the file menu. Exit by choosing }{\b\insrsid8742607 exit}{\insrsid8742607  from the file menu.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 44.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 view}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to get a preview. (}{\b\insrsid8742607 viewx}{\insrsid8742607  gives previews of the command }{\b\insrsid8742607 plotx}{\insrsid8742607  which plots expansions automatically).

\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 45.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If you need to correct something type }{\b\insrsid8742607 edg}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 , now you will see a grey window with several grey buttons. Here you can adjust almost everything that is related to plotting.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 46.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If the spectrum looks right, type }{\b\insrsid8742607 plot}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 . The spectrum will now be printed on one of the printers in the NMR lab.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 47.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Press the}{\b\insrsid8742607  Spin}{\insrsid8742607  }{\b\insrsid8742607 on/off }{\insrsid8742607 button to off and then the }{\b\insrsid8742607 Lock on/off }{\insrsid8742607 button to off.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 48.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Eject sample with the }{\b\insrsid8742607 Lift on/off }{\insrsid8742607 button on the shim console and remove your sample from spinner and reinsert the standard sample and lower it by pressing }{\b\insrsid8742607 Lift on/off}{\insrsid8742607  and type }{
\b\insrsid8742607 lock cdcl3}{\insrsid8742607  and see that the instrument locks in the lock window.  Press }{\b\insrsid8742607 Spin on.}{\insrsid8742607  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs20\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 49.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 delp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  and a list of all your experiments on the v disk (u if you run on your home directory) comes up, click on all experiments where there is not said \'93no processed data\'94
.  Then click on }{\b\insrsid8742607 execute}{\insrsid8742607 .  Do not click on delete all, you might loose all data including acquisition data if you do this.  }{\b\insrsid8742607 delp}{\insrsid8742607 
 (delete processed data) kills all processed data and helps conserve disk space.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 50.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 wrd}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   this is the command for writing the dataset to another disk.  Usually there is no need for th
is since USIT is taking backup copies every second from all of the hard disks in the nmr lab.  Go to 62 if you do not want to save the dataset.  Continue as follows if you want a copy on another disk.  
\par }\pard \qj \fi360\li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 Enter target data set }{\b\insrsid8742607 NAME:}{\insrsid8742607 \tab \tab \tab }{\b\insrsid8742607 FR5043II}{
\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607 \tab \tab }{\insrsid8742607 (use your own expname)}{\b\insrsid8742607 
\par }\pard \qj \li720\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin720\itap0 {\insrsid8742607 Enter target data set}{\b\insrsid8742607  EXPNO:\tab \tab 2}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607 \tab \tab \tab }{
\insrsid8742607 (use the expno seen in the top part of the xwinnmr window).
\par Enter target data set }{\b\insrsid8742607 PROCNO:\tab \tab 1}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607 \tab \tab \tab }{\insrsid8742607 (use the procno seen in the top part of the xwinnmr window).
\par }\pard \qj \fi-3600\li4320\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin4320\itap0 {\insrsid8742607 Enter target disk unit }{\b\insrsid8742607 DU}{\insrsid8742607 :\tab }{\b\insrsid8742607 M:}{\b\f3\fs28\insrsid8742607 \'20\'bf}{
\insrsid8742607  \tab The data set will go to your home directory.  }{\fs20\insrsid8742607 The available disks are: C: and M:.}{\insrsid8742607 
\par }\pard \qj \fi360\li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 Enter target user name }{\b\insrsid8742607 USER}{\insrsid8742607 :\tab }{\b\insrsid8742607 UIO-username}{\b\f3\fs28\insrsid8742607 
\'bf}{\b\insrsid8742607  \tab }{\insrsid8742607 (your own uio user name)
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 51.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
The dataset is now copied.  If you want to move expno 2, 3, 4, 11, 12 or whatever expno you have used - get each dataset in the Xwinnmr window (}{\b\insrsid8742607 re 11}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
 moves expno 11 into the window for instance) and }{\b\insrsid8742607 wrd}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  it away.}{\fs18\insrsid8742607 
\par }\pard \qj \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 52.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on the }{\b\insrsid8742607 quit}{\insrsid8742607  button in the }{\b\insrsid8742607 lock display}{\insrsid8742607  with the left mouse button.  The next user will not be able to open the lock display if you forget this.}{\fs18\insrsid8742607 
\par }\pard \qj \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 53.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type}{\b\insrsid8742607  kill}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  in the xwinnmr window.  If some xwinnmr processes are running you will get a list.  It is especially important to kill the lock displa
y if it is on the list.  Click on the lock display in the list.  If the lock display is not completely removed before logging out the next user will be unable to open the lock display.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 54.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If you are satisfied with the result press }{\b\insrsid8742607 exit}{\insrsid8742607  under }{\b\insrsid8742607 File}{\insrsid8742607  and }{\b\insrsid8742607 OK}{\insrsid8742607  in CPR window which appears.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 55.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls12\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Select }{\b\insrsid8742607 log out}{\insrsid8742607  from the start menu to log out of the computer.
\par }\pard \ql \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 \page }{\b\fs36\up6\insrsid8742607 31}{\b\fs36\insrsid8742607 P and }{\b\fs36\up6\insrsid8742607 19}{\b\fs36\insrsid8742607 
F and NMR at DPX200 and }{\b\fs36\up6\insrsid8742607 15}{\b\fs36\insrsid8742607 N and }{\b\fs36\up6\insrsid8742607 31}{\b\fs36\insrsid8742607 P NMR DPX300 with the QNP probes. 
\par }\pard \qc \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 Version 1
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par }\pard \qj \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\insrsid8742607 When the quadruple (4 nuclei) probes are inside the magnets it is very simple to acquire }{\up6\insrsid8742607 31}{\insrsid8742607 P and }{
\up6\insrsid8742607 19}{\insrsid8742607 F on the 200 MHz spectrometer and }{\up6\insrsid8742607 15}{\insrsid8742607 N (not so easy) and }{\up6\insrsid8742607 31}{\insrsid8742607 P on the 300 MHz spectrometer.  Almost everything is identical to }{
\up6\insrsid8742607 1}{\insrsid8742607 H and }{\up6\insrsid8742607 13}{\insrsid8742607 C acquisition.  You must select the new nuclei with }{\b\insrsid8742607 rpar,}{\insrsid8742607  initialize with }{\b\insrsid8742607 ii}{\insrsid8742607 
 and lock on the correct solvent.  Each time you select new parameters (and nuclei) with }{\b\insrsid8742607 rpar}{\insrsid8742607  you must }{\b\insrsid8742607 lock}{\insrsid8742607 
 on the correct solvent.  The instruments does not remember the solvent you locked on initially when a new }{\b\insrsid8742607 rpar}{\insrsid8742607  is performed.  Each }{\b\insrsid8742607 rpar}{\insrsid8742607  file is for 
a specific solvent the engineer used when installing the instrument and checking the different nuclei.  So you can get an acetone setup when changing to }{\up6\insrsid8742607 31}{\insrsid8742607 P with }{\b\insrsid8742607 rpar QNP.31P}{\insrsid8742607 
 even if you just run a }{\up6\insrsid8742607 1}{\insrsid8742607 H experiment in CDCl}{\dn4\insrsid8742607 3}{\insrsid8742607 .  }{\b\insrsid8742607 Lock cdcl3}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  fixes this after }{\b\insrsid8742607 rpar}{
\insrsid8742607 !
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par }\pard \ql \fi360\li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\b\fs28\up6\insrsid8742607 15}{\b\fs28\insrsid8742607 N NMR with and without }{\b\fs28\up6\insrsid8742607 1}{\b\fs28\insrsid8742607 
H decoupling at DPX300.
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\b\fs28\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 1.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\b\insrsid8742607 
Login}{\insrsid8742607 , }{\b\insrsid8742607 edc}{\insrsid8742607 , }{\b\insrsid8742607 spinning off}{\insrsid8742607 , }{\b\insrsid8742607 lock off}{\insrsid8742607 , }{\b\insrsid8742607 eject standard sample}{\insrsid8742607 , }{\b\insrsid8742607 
insert your sample, spinning on }{\insrsid8742607 and }{\b\insrsid8742607 rsh}{\insrsid8742607  as described in }{\up6\insrsid8742607 1}{\insrsid8742607 H and }{\up6\insrsid8742607 13}{\insrsid8742607 C manuals.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 2.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 rpar }{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'2e}{\b\f3\fs28\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 3.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on }{\b\insrsid8742607 N15}{\insrsid8742607  with the left mouse button to get parameters for }{\up6\insrsid8742607 15}{\insrsid8742607 N with coupling to protons.  Click on }{\b\insrsid8742607 N15IG}{\insrsid8742607 
 with the left mouse button to get parameters for }{\up6\insrsid8742607 15}{\insrsid8742607 N with decoupling of protons. Press }{\b\insrsid8742607 copy all.}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 4.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 getprosol}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 5.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 edasp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 \tab edit spectrometer (a window showing the logical setup of the radio transmitter etc. comes up - see if }{\up6\insrsid8742607 15}{\insrsid8742607 
N is selected under NUC1 and NUC2 is off when you chose rpar 15N and that NUC2 is 1H for rpar 15N}{\insrsid4994597 IG}{\insrsid8742607 .  Click on }{\b\insrsid8742607 save. }{\insrsid8742607  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 6.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 lock}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607  }{\insrsid8742607 and click with the left mouse button}{\b\insrsid8742607  }{\insrsid8742607 on the ap
propriate solvent.  No need to shim if you did this earlier on the same sample and have not removed and inserted it again in the magnet.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 7.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'20}{\insrsid8742607 and listen carefully.  A clear sound shall come from the underside of the magnet in about 20 seconds when the pneumatic switcher is changing to}{
\insrsid4994597  15N.}{\insrsid8742607   Confirm that the button/light marked manual at the right side of the box at bottom of the box at the left magnet leg is off.  If the light is on on the button press it until it is off (2-4 times) and repeat  }{
\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\fs28\insrsid8742607 \'2e\'20}{\b\f3\fs28\insrsid8742607 \'20}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 8.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 rga}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'2e}{\b\f3\fs28\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 9.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 ns}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to check number of scans and }{\b\insrsid8742607 d1}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to check the relaxation delay.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 10.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 zg}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'2e}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 11.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Continue as with }{\up6\insrsid8742607 1}{\insrsid8742607 H and }{\up6\insrsid8742607 13}{\insrsid8742607 C acquisition.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 12.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls13\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Remember to type}{\b\insrsid8742607  kill}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  in th
e xwinnmr window before logging out.  If some xwinnmr processes are running you will get a list.  It is especially important to kill the lock display if it is on the list.  Click on the lock display in the list.  If the lock display is not completely remo
ved before logging out the next user will be unable to open the lock display.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par \page 
\par }\pard \qc \li360\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin360\itap0 {\b\fs28\up6\insrsid8742607 19}{\b\fs28\insrsid8742607 F NMR with }{\b\fs28\up6\insrsid8742607 1}{\b\fs28\insrsid2060349 H coupling at DPX200}{
\b\fs28\insrsid8742607 
\par }{\fs20\insrsid8742607 Version 1}{\b\fs28\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 1.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\b\insrsid8742607 
Login}{\insrsid8742607 , }{\b\insrsid8742607 edc}{\insrsid8742607 , }{\b\insrsid8742607 spinning off}{\insrsid8742607 , }{\b\insrsid8742607 lock off}{\insrsid8742607 , }{\b\insrsid8742607 eject standard sample}{\insrsid8742607 , }{\b\insrsid8742607 
insert your sample, spinning on }{\insrsid8742607 and }{\b\insrsid8742607 rsh}{\insrsid8742607  as described in }{\up6\insrsid8742607 1}{\insrsid8742607 H and }{\up6\insrsid8742607 13}{\insrsid8742607 C manuals.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 2.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 rpar}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'2e}{\b\f3\fs28\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 3.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Click on }{\b\insrsid8742607 F19}{\insrsid8742607  with left mouse button to get parameters for 19F with coupling to protons.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 4.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 getprosol}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 5.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 edasp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 \tab edit spectrometer - a window showing the logical setup of the radio transmitter etc. comes up - see if }{\up6\insrsid8742607 19}{\insrsid8742607 
F is selected under NUC1 and NUC2 is off.  Click on }{\b\insrsid8742607 save. }{\insrsid8742607  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 6.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 lock}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607  }{\insrsid8742607 and click with the left mouse button}{\b\insrsid8742607  }{\insrsid8742607 
on the appropriate solvent.  No need to shim if you did this earlier on the same sample and have not removed and inserted it again in the magnet.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 7.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'20}{\insrsid8742607 and listen carefully.  A clear sound shall come from the underside of the magnet in about 20 seconds when the pneumatic switcher is changing to }{
\up6\insrsid8742607 19}{\insrsid8742607 F.  Confirm that the button/light marked manual at the right side of the box at bottom of the box at the left magnet leg is off.  If the light is on on the button press it until it is off (2-4 times) and repeat  }{
\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\fs28\insrsid8742607 \'2e\'20}{\b\f3\fs28\insrsid8742607 \'20}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 8.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 rga}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'2e}{\b\f3\fs28\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\b\f3\fs28\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 9.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 ns}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to check number of scans and }{\b\insrsid8742607 d1}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to check the relaxation delay.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 10.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 zg}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'2e}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 11.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Continue as with }{\up6\insrsid8742607 1}{\insrsid8742607 H and }{\up6\insrsid8742607 13}{\insrsid8742607 C acquisition.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 12.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Sometimes the 19F resonances are outside the ppm area chosen by the spectrometer. Increase the width by typing }{\b\insrsid8742607 sw}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  and type in a larger number.  Go back to 7.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 13.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls16\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Remember to type}{\b\insrsid8742607  kill}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
 in the xwinnmr window before logging out.  If some xwinnmr processes are running you will get a list.  It is especially important to kill the lock display if it is on the list.  Click on the lock display in the list.  If the loc
k display is not completely removed before logging out the next user will be unable to open the lock display.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 \page }{\b\fs28\up6\insrsid8742607 31}{\b\fs28\insrsid8742607 P NMR with and without }{\b\fs28\up6\insrsid8742607 1}{
\b\fs28\insrsid8742607 H decoupling at DPX 200 and DPX 300.
\par }{\fs20\insrsid8742607 Version 1
\par }{\b\fs28\insrsid8742607 
\par {\listtext\pard\plain\b\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 1.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\b\insrsid8742607 Login}{\insrsid8742607 , }{\b\insrsid8742607 edc}{\insrsid8742607 , }{\b\insrsid8742607 spinning off}{\insrsid8742607 , }{\b\insrsid8742607 lock off}{\insrsid8742607 , }{\b\insrsid8742607 eject standard sample}{\insrsid8742607 , }{
\b\insrsid8742607 insert your sample}{\insrsid8742607 , }{\b\insrsid8742607 spinning on }{\insrsid8742607 and }{\b\insrsid8742607 rsh}{\insrsid8742607  as described in }{\up6\insrsid8742607 1}{\insrsid8742607 H and }{\up6\insrsid8742607 13}{
\insrsid8742607 C manuals.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 2.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Type }{\b\insrsid8742607 rpar}{\b\f3\fs28\insrsid8742607 \'bf}{\f3\insrsid8742607 \'2e}{\f3\insrsid77361 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0\pararsid77361 {\f3\insrsid77361 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid77361\charrsid77361 \hich\af0\dbch\af0\loch\f0 3.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 
{\insrsid77361\charrsid77361 Type }{\b\insrsid77361\charrsid77361 getprosol}{\b\f3\fs28\insrsid77361 \'bf\'2e}{\f3\insrsid77361\charrsid77361 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 4.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Click on }{\b\insrsid8742607 P31}{\insrsid8742607  with left mouse button to get parameters for }{\up6\insrsid8742607 31}{\insrsid8742607 P with coupling to protons, or click on }{\b\insrsid8742607 P31cpd}{\insrsid8742607 
 with the left mouse button to get parameters for }{\up6\insrsid8742607 31}{\insrsid8742607 P with }{\up6\insrsid8742607 1}{\insrsid8742607 H decoupling. 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 5.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 On DPX 200 type }{\b\insrsid8742607 edasp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  edit spectrometer - a window showing the logical setup of the radio transmitter etc. comes up.  Click on }{\b\insrsid8742607 save.}{
\insrsid8742607   
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 6.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Type }{\b\insrsid8742607 lock}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607  }{\insrsid8742607 and click with the left mouse button}{\b\insrsid8742607  }{\insrsid8742607 
on the appropriate solvent.  No need to shim if you did this earlier on the same sample and have not removed and inserted it again in the magnet.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 7.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Type }{\b\insrsid8742607 ii}{\b\f3\fs28\insrsid8742607 \'bf}{\b\f3\fs28\insrsid77361 \'2c}{\b\fs28\insrsid77361\charrsid77361  }{\insrsid77361\charrsid77361 press }{\b\insrsid77361\charrsid77361 seen}{\insrsid77361\charrsid77361  in}{
\insrsid77361  the window that appears, }{\insrsid8742607\charrsid77361 \u-4064\'3f}{\insrsid8742607 and listen carefully. A clear sound shall come in about 2}{\insrsid77361 0 seconds from the underside of }{\insrsid8742607 
the magnet when the pneumatic switcher is changing to }{\up6\insrsid8742607 31}{\insrsid8742607 
P.  Confirm that the button/light marked manual at the right side of the box at bottom of the box at the left magnet leg is off.  If the light is on on the button press it until it is off (2-4 times) and repeat  }{\b\insrsid8742607\charrsid77361 ii}{
\b\f3\fs28\insrsid8742607\charrsid77361 \'bf}{\f3\fs28\insrsid8742607\charrsid77361 \'2e}{\insrsid8742607\charrsid77361 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607\charrsid77361 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607\charrsid77361 \hich\af0\dbch\af0\loch\f0 8.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar
\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {\insrsid8742607\charrsid77361 T}{\insrsid8742607 ype }{\b\insrsid8742607 rga}{\b\f3\fs28\insrsid8742607 \'bf
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\b\f3\fs28\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 9.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Type }{\b\insrsid8742607 ns}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to check number of scans and }{\b\insrsid8742607 d1}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  to check the relaxation delay.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 10.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Type }{\b\insrsid8742607 zg}{\b\f3\fs28\insrsid8742607 \'2e}{\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 11.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Continue as with }{\up6\insrsid8742607 1}{\insrsid8742607 H and }{\up6\insrsid8742607 13}{\insrsid8742607 C acquisition.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af0\dbch\af0\loch\f0 12.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls31\adjustright\rin0\lin720\itap0\pararsid77361 {
\insrsid8742607 Remember to type}{\b\insrsid8742607  kill}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  in the xwinnmr window before logging out.  If some xwinnmr processes are running you will get a list.  It is especially important to kill the lock 
}{\insrsid2060349 display if it is on the list.  C}{\insrsid8742607 lick on the lock display in the list.  If the lock display is not completely removed before logging out the next user will be unable to open the lock display.  
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\fs18\insrsid8742607 
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 \page }{\b\fs36\insrsid8742607 Saving and transferring data from DPX200 or DPX300 to your home directory or another disk. }{\b\insrsid8742607 

\par }{\b\fs36\insrsid8742607 Remote login and processing.  
\par }{\insrsid8742607 Version 1
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par }{\b\insrsid8742607 HOW TO TRANSFER DATA ACQUIRED BY YOURSELF TO YOUR OWN HOME DIRECTORY 
\par }\pard \qc \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\b\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 1.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls19\adjustright\rin0\lin720\itap0 {\insrsid8742607 
It is recommended that you delete processed data and only store data at one disk.  Type }{\b\insrsid8742607 delp}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  and a list of all your experiments on the }{\b\insrsid6883174 D}{\b\insrsid8742607 :}{
\insrsid8742607  disk you have selected comes up.  Click on all experiments where there is not said \'93no processed data\'94.  Then click on }{\b\insrsid8742607 execute}{\insrsid8742607 
.  Do not click on delete all, you might loose all data including acquisition data if you do this.  }{\b\insrsid8742607 delp}{\insrsid8742607  (delete processed data) kills all processed data and helps conserve disk space.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 2.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls19\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Type }{\b\insrsid8742607 wrd}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607   this is the command for writing the dataset which is on screen to another disk (home or other place) for permanent storage.  
\par }\pard \qj \fi720\li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 Enter target data set }{\b\insrsid8742607 NAME:}{\insrsid8742607 \tab \tab \tab }{\b\insrsid8742607 FR5043II}{\b\f3\fs28\insrsid8742607 
\'bf}{\b\insrsid8742607 \tab \tab }{\insrsid8742607 (use your own expname)}{\b\insrsid8742607 
\par }\pard \qj \li720\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin720\itap0 {\insrsid8742607 Enter target data set}{\b\insrsid8742607  EXPNO:\tab \tab 1}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607 \tab \tab \tab }{
\insrsid8742607 (use the expno seen in the top part of the xwinnmr window).
\par Enter target data set }{\b\insrsid8742607 PROCNO:\tab \tab 1}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607 \tab \tab \tab }{\insrsid8742607 (use the procno seen in the top part of the xwinnmr window).
\par Enter target disk unit }{\b\insrsid8742607 DU}{\insrsid1518156 :\tab \tab \tab }{\b\insrsid6883174 D}{\b\insrsid8742607 :}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  \tab \tab The data set will go to the hard disk.  }{\fs20\insrsid8742607 
The available disks are: C: }{\fs20\insrsid6883174 D: }{\fs20\insrsid8742607 and M:.}{\insrsid8742607 
\par Enter target user name }{\b\insrsid8742607 USER}{\insrsid8742607 :\tab \tab }{\b\insrsid8742607 UIO-username}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607  \tab }{\insrsid8742607 (your own uio user name)
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 3.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls19\adjustright\rin0\lin720\itap0 {\insrsid8742607 
The dataset is now copied.  If you want to move expno 2, 3, 4, 11, 12 or whatever expno you have used - get each dataset in the Xwinnmr window (}{\b\insrsid8742607 re 11}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607 
 moves expno 11 into the window for instance) and }{\b\insrsid8742607 wrd}{\b\f3\fs28\insrsid8742607 \'bf}{\insrsid8742607  it away.}{\fs20\insrsid8742607 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 4.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls19\adjustright\rin0\lin720\itap0 {\b\insrsid8742607 
Only data sets which are in the xwinnmr window can be moved.  }{\insrsid8742607 When you have moved EXPNO 1 you must }{\b\insrsid8742607 append}{\insrsid8742607  and }{\b\insrsid8742607 apply}{\insrsid8742607 
 the next one(using the search window) into the xwinnmr window, then you can move this one with }{\b\insrsid8742607 wrd}{\insrsid8742607 .  This takes a little time 
when sending a whole Set and Run experiment home - but it works fine and there will be no trouble with who owns the dataset and permission problems will not arise with data sets copied this way.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 5.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls19\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Delete the original dataset. Use the command }{\b\insrsid8742607 del}{\b\f3\fs28\insrsid8742607 \'bf}{\b\insrsid8742607  }{\insrsid8742607 . 
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 6.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls19\adjustright\rin0\lin720\itap0 {\insrsid8742607 
If you later wants to work on the moved dataset use }{\b\insrsid8742607 search}{\insrsid8742607  to find it, then }{\b\insrsid8742607 append}{\insrsid8742607  and }{\b\insrsid8742607 apply}{\insrsid8742607  it to the xwinnmr window, }{\b\insrsid8742607 
efp}{\insrsid8742607  or }{\b\insrsid8742607 xfb}{\insrsid8742607  (2D dataset) to Fourier transform it.  If the computer you are using does have another plotter attached use }{\b\insrsid8742607 edo}{\insrsid8742607  (edit output) 
to select the new plotter.  The data set does regretfully remember the plotter name connected to the computer used to acquire the spectrum.  }{\b\insrsid8742607 edg }{\insrsid8742607 must be used if you are working on 2D\rquote 
s to select EDPROJ1 and in the sub menu PF1EXT (external), PF1DU (disk), 
PF1USER (your unix user name), PF1NAME (expname), PF1EXP (expno), PF1PROC (procno usually 1) to get the correct projection on the F1 axis.  EDPROJ2 with the sub menu containing PF2EXT, PF2DU, PF2USER, PF2NAME, PF2EXP, PF2PROC selections are used to get th
e correct projection on the F2 axis on the 2D spectrum.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par {\listtext\pard\plain\f37\lang2057\langfe1033\langnp2057\insrsid8742607 \hich\af37\dbch\af0\loch\f37 7.\tab}}\pard \qj \fi-360\li720\ri0\sl360\slmult0\widctlpar\jclisttab\tx720\aspalpha\aspnum\faauto\ls19\adjustright\rin0\lin720\itap0 {\insrsid8742607 
Exit and logout.
\par }\pard \qj \li0\ri0\sl360\slmult0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par }\pard \ql \li0\ri0\widctlpar\aspalpha\aspnum\faauto\adjustright\rin0\lin0\itap0 {\insrsid8742607 
\par }}